2-phenylpropenyl chloride
2-phenylpropenyl chloride
CAS: 22414-26-2
Molecular Formula: C9H9ClO
2-phenylpropenyl chloride - Names and Identifiers
| Name | 2-phenylpropenyl chloride |
| Synonyms | 2-phenylpropenyl chloride 2-phenylpropanoyl chloride 2-Phenyl-propionyl chloride Benzeneacetyl chloride, α-methyl- |
| CAS | 22414-26-2 |
2-phenylpropenyl chloride - Physico-chemical Properties
| Molecular Formula | C9H9ClO |
| Molar Mass | 168.62 |
| Density | 1.139±0.06 g/cm3(Predicted) |
| Melting Point | 112-114 °C(Solv: ligroine (8032-32-4); dichloromethane (75-09-2)) |
| Boling Point | 98-100 °C(Press: 15 Torr) |
| BRN | 1938154 |
| Storage Condition | 2-8℃ |
2-phenylpropenyl chloride - Risk and Safety
| Hazard Symbols | C - Corrosive |
| Risk Codes | 34 - Causes burns |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection. S45 - In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.) |
| UN IDs | UN 3265 8 / PGII |
| WGK Germany | 3 |
2-phenylpropenyl chloride - Introduction
2-phenylpropylchloride (2-phenylpropylchloride) is an organic compound with the chemical formula C9H9Cl. The following is a description of its nature, use, preparation and safety information:
Nature:
-Appearance: 2-phenylpropyl chloride is a colorless to pale yellow liquid.
-Solubility: It is soluble in many organic solvents, such as ethanol, chloroform and dichloromethane.
Use:
-2-phenylpropyl chloride is commonly used as an important reagent and intermediate in organic synthesis, and is used to synthesize a variety of drugs and chemical substances.
-It can be used for the synthesis of phenylacetone, coumarin compounds, amino acids and peptides.
Method:
The preparation method of 2-phenylpropyl chloride is usually obtained by reacting phenylacetone with thionyl chloride. The specific steps are as follows:
1. Under appropriate reaction conditions, phenyl acetone is dissolved in thionyl chloride.
2. Stir the reaction at an appropriate temperature for a period of time to complete the reaction.
3. The inorganic salt in the reaction mixture is removed by an appropriate method.
4. The pure 2-phenylpropylyl chloride product is obtained by distillation or other purification methods.
Safety Information:
-2-phenylpropyl chloride is a pungent odor compound that is irritating to the eyes, skin and respiratory tract. Necessary safety measures should be taken during handling and use, including wearing appropriate protective clothing, gloves and breathing apparatus.
-When stored, it should be kept away from fire and oxidants, and stored in a cool, well-ventilated place.
-When disposing of waste, it should be disposed of in accordance with local regulations to avoid pollution to the environment.
Nature:
-Appearance: 2-phenylpropyl chloride is a colorless to pale yellow liquid.
-Solubility: It is soluble in many organic solvents, such as ethanol, chloroform and dichloromethane.
Use:
-2-phenylpropyl chloride is commonly used as an important reagent and intermediate in organic synthesis, and is used to synthesize a variety of drugs and chemical substances.
-It can be used for the synthesis of phenylacetone, coumarin compounds, amino acids and peptides.
Method:
The preparation method of 2-phenylpropyl chloride is usually obtained by reacting phenylacetone with thionyl chloride. The specific steps are as follows:
1. Under appropriate reaction conditions, phenyl acetone is dissolved in thionyl chloride.
2. Stir the reaction at an appropriate temperature for a period of time to complete the reaction.
3. The inorganic salt in the reaction mixture is removed by an appropriate method.
4. The pure 2-phenylpropylyl chloride product is obtained by distillation or other purification methods.
Safety Information:
-2-phenylpropyl chloride is a pungent odor compound that is irritating to the eyes, skin and respiratory tract. Necessary safety measures should be taken during handling and use, including wearing appropriate protective clothing, gloves and breathing apparatus.
-When stored, it should be kept away from fire and oxidants, and stored in a cool, well-ventilated place.
-When disposing of waste, it should be disposed of in accordance with local regulations to avoid pollution to the environment.
Last Update：2024-04-09 02:00:44
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CAS: 22414-26-2
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